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化学和生化试剂
高端化学
配体
手性配体
(R)-(-)-联萘酚磷酸酯

(R)-(-)-联萘酚磷酸酯

规格或纯度: 98%

CAS编号: 39648-67-4
分子式: C₂₀H₁₃O₄P
分子量: 348.29
Beilstein号: 4713363
MDL号: MFCD00010045
PubChem编号: 99589

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货号 (SKU)	包装规格	是否现货	价格	数量
B107410-250mg	250mg	现货
B107410-1g	1g	现货
B107410-5g	5g	现货
B107410-10g	10g	现货
B107410-25g	25g	现货
B107410-100g	100g	现货

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不对称合成磷化合物

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基本描述

规格或纯度	98%
英文名称	(R)-(-)-BNP acid
别名	R-联萘酚磷酸酯\|(R)-(-)-1,1'-联萘-2,2'-二基磷酸氢酯, (R)-4-羟基二萘并[2,1-d:1',2'-f][1,3,2]二噁磷杂庚英-4-氧化物\|(R)-(-)-1,1'-联萘基-2,2'-双磷酸氢酯\|(R)-(-)-2,2'-二羟基-1,1'-联萘磷酸酯
英文别名	39648-67-4\|35193-64-7\|35193-63-6\|1,1'-Binaphthyl-2,2'-diyl hydrogenphosphate\|(R)-(-)-1,1'-Binaphthyl-2,2'-diyl hydrogenphosphate\|(S)-(+)-1,1'-Binaphthyl-2,2'-diyl hydrogenphosphate\|(11bS)-4-Hydroxydinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepine 4-oxide\|(R
运输条件	常规运输
备注	250mg卖完停产，不再备货
产品介绍	氢羧基化反应中作为手性配体；在异构体选择性的mannich反应中，用作手性bronsted酸催化剂。

名称和标识符

IUPAC Name	13-hydroxy-12,14-dioxa-13λ5-phosphapentacyclo[13.8.0.02,11.03,8.018,23]tricosa-1(15),2(11),3,5,7,9,16,18,20,22-decaene 13-oxide
INCHI	InChI=1S/C20H13O4P/c21-25(22)23-17-11-9-13-5-1-3-7-15(13)19(17)20-16-8-4-2-6-14(16)10-12-18(20)24-25/h1-12H,(H,21,22)
InChi Key	JEHUZVBIUCAMRZ-UHFFFAOYSA-N
Canonical SMILES	C1=CC=C2C(=C1)C=CC3=C2C4=C(C=CC5=CC=CC=C54)OP(=O)(O3)O
WGK Germany	3
PubChem CID	99589
分子量	348.29
Beilstein号	4713363
Reaxy-Rn	2014273

化学和物理性质

溶解性	Solubility in hot Methanol, almost transparency.
密度	1.49
比旋光度	-595 ° (C=1, MeOH)

安全和危险性（GHS）

象形图	Harmful
信号词	Warning
危险声明	H315: Causes skin irritation H319: Causes serious eye irritation H335: May cause respiratory irritation
预防措施声明	P261,P305+P351+P338,P280,P302+P352,P321,P405,P501,P264,P271,P304+P340,P403+P233,P362+P364,P264+P265,P337+P317,P332+P317,P319
WGK Germany	3
Reaxy-Rn	2014273
个人防护装备	dust mask type N95 (US),Eyeshields,Gloves

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FAQ

手性磷酸——用途广泛的多功能有机催化剂

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标签:

催化剂有机催化剂手性磷酸还原胺化丙烯基化烷基化

Chiral Phosphoric Acids——Versatile Organocatalysts with Expanding Applications

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Catalyst Organocatalyst chiral phosphoric acids reductive amination allylation alkylation

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参考文献

1. Y Mechref,Z El Rassi. (1997-06-01) Comparison of alkylglycoside surfactants in enantioseparation by capillary electrophoresis.. Electrophoresis, 18 ((6)): (912-918). [PMID:9221877]
2. M E McCarroll,F H Billiot,I M Warner. (2001-07-18) Fluorescence anisotropy as a measure of chiral recognition.. Journal of the American Chemical Society, 123 ((13)): (3173-3174). [PMID:11457044]
3. Tom M H Choy,Wing-Hong Chan,Albert W M Lee,Carmen W Huie. (2003-10-01) Stacking and separation of enantiomers by acetonitrile-salt mixtures in micellar electrokinetic chromatography.. Electrophoresis, 24 ((18)): (3116-3123). [PMID:14518033]
4. Ulrich Schmitt,Mevlut Ertan,Ulrike Holzgrabe. (2004-09-08) Chiral capillary electrophoresis: facts and fiction on the reproducibility of resolution with randomly substituted cyclodextrins.. Electrophoresis, 25 ((16)): (2801-2807). [PMID:15352012]
5. Kevin F Morris,Bridget A Becker,Bertha C Valle,Isiah M Warner,Cynthia K Larive. (2006-09-01) Use of NMR binding interaction mapping techniques to examine interactions of chiral molecules with molecular micelles.. The journal of physical chemistry. B, 110 ((35)): (17359-17369). [PMID:16942071]
6. Dorothee Wistuba,Anja Bogdanski,Kim L Larsen,Volker Schurig. (2006-10-06) Delta-cyclodextrin as novel chiral probe for enantiomeric separation by electromigration methods.. Electrophoresis, 27 ((21)): (4359-4363). [PMID:17022018]
7. Alicia A Williams,Sayo O Fakayode,Xiaodong Huang,Isiah M Warner. (2006-11-01) Use of multivariate analysis for optimization of separation parameters and prediction of migration time, resolution, and resolution per unit time in micellar electrokinetic chromatography.. Electrophoresis, 27 ((21)): (4127-4140). [PMID:17075942]
8. Masahiro Yamanaka,Junji Itoh,Kohei Fuchibe,Takahiko Akiyama. (2007-05-05) Chiral Br?nsted acid catalyzed enantioselective Mannich-type reaction.. Journal of the American Chemical Society, 129 ((21)): (6756-6764). [PMID:17477527]
9. Simon M Mwongela,Noreen Siminialayi,Kristin A Fletcher,Isiah M Warner. (2007-07-12) A comparison of ionic liquids to molecular organic solvents as additives for chiral separations in micellar electrokinetic chromatography.. Journal of separation science, 30 ((9)): (1334-1342). [PMID:17623476]
10. Eugene Billiot,Fereshteh Billiot,Isiah M Warner. (2008-11-15) Optimization of 12 chiral analytes with 8 polymeric surfactants.. Journal of chromatographic science, 46 ((9)): (757-763). [PMID:19007474]
11. Jun He,Shahab A Shamsi. (2008-12-27) Multivariate approach for the enantioselective analysis in micellar electrokinetic chromatography-mass spectrometry. I. Simultaneous optimization of binaphthyl derivatives in negative ion mode.. Journal of chromatography. A, 1216 ((5)): (845-856). [PMID:19110258]
12. Ke Shen,Xiaohua Liu,Yunfei Cai,Lili Lin,Xiaoming Feng. (2009-05-07) Facile and efficient enantioselective Strecker reaction of ketimines by chiral sodium phosphate.. Chemistry (Weinheim an der Bergstrasse, Germany), 15 ((24)): (6008-6014). [PMID:19418513]
13. Yingying Dong,Linda B McGown. (2011-06-28) Chiral selectivity of guanosine media in capillary electrophoresis.. Electrophoresis, 32 ((13)): (1735-1741). [PMID:21706497]
14. Ioannis J Stavrou,Constantina P Kapnissi-Christodoulou. (2012-12-05) Use of chiral amino acid ester-based ionic liquids as chiral selectors in CE.. Electrophoresis, 34 ((4)): (524-530). [PMID:23208781]
15. Christine M Hebling,Laura E Thompson,Kyle W Eckenroad,Gregory A Manley,Roderick A Fry,Karl T Mueller,Timothy G Strein,David Rovnyak. (2008-12-05) Sodium cholate aggregation and chiral recognition of the probe molecule (R,S)-1,1'-binaphthyl-2,2'-diylhydrogenphosphate (BNDHP) observed by 1H and 31P NMR spectroscopy.. Langmuir : the ACS journal of surfaces and colloids, 24 ((24)): (13866-13874). [PMID:19053628]

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