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N-羟基邻苯二甲酰亚胺(NOP)

规格或纯度: 98%
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货号 (SKU) 包装规格 是否现货 价格 数量
H106354-25g
 25g 现货 Stock Image
H106354-100g
 100g 现货 Stock Image
H106354-250g
 250g 现货 Stock Image
H106354-500g
 500g 现货 Stock Image
H106354-2.5kg
 2.5kg 现货 Stock Image
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官能团化合物 酰亚胺
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基本描述

规格或纯度 98%
英文名称 N-Hydroxyphthalimide
别名 N-羟基酞酰亚胺
英文别名 N-HYDROXYPHTHALIMIDE|524-38-9|2-hydroxyisoindoline-1,3-dione|2-Hydroxy-1H-isoindole-1,3(2H)-dione|2-Hydroxyphthalimide|1H-Isoindole-1,3(2H)-dione, 2-hydroxy-|Phthalimide, N-hydroxy-|2-hydroxyisoindole-1,3-dione|2-oxidanylisoindole-1,3-dione|BXI99M81X0|CHE
运输条件 常规运输
产品介绍

用作阿米卡星等药物中间体。制备胺核苷，以用于偶联反应生成非阴离子反义寡聚核苷.

名称和标识符

EC号 208-358-1
IUPAC Name 2-hydroxyisoindole-1,3-dione
INCHI InChI=1S/C8H5NO3/c10-7-5-3-1-2-4-6(5)8(11)9(7)12/h1-4,12H
InChi Key CFMZSMGAMPBRBE-UHFFFAOYSA-N
Canonical SMILES C1=CC=C2C(=C1)C(=O)N(C2=O)O
WGK Germany 3
RTECS TI5200000
PubChem CID 10665
分子量 163.13
Beilstein号 131208
Reaxy-Rn 131208

化学和物理性质

溶解性 Slightly soluble in water.
密度 1.638
熔点 233-235°C

安全和危险性（GHS）

象形图
ghs07

Harmful
信号词 Warning
危险声明 H315: Causes skin irritation
H319: Causes serious eye irritation
H335: May cause respiratory irritation
预防措施声明 P261,P305+P351+P338,P280,P302+P352,P321,P405,P501,P264,P271,P304+P340,P403+P233,P362+P364,P264+P265,P337+P317,P332+P317,P319
WGK Germany 3
RTECS TI5200000
Reaxy-Rn 131208
个人防护装备 dust mask type N95 (US),Eyeshields,Gloves

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参考文献

1. S Fregert,K Gustafsson,L Trulsson.  (1983-01-01)  Contact allergy to N-hydroxyphthalimide..  Contact dermatitis,  9  ((1)):  (84-85).  [PMID:6220864]
2. James M Takacs,Scott D Schroeder,Jianxin Han,Meg Gifford,Xun-Tian Jiang,Twana Saleh,Suresh Vayalakkada,Amy H Yap.  (2003-09-26)  Controlling mode selectivity in palladium-catalyzed bisdiene carbocyclizations: optimizing for cyclization-trapping over cycloisomerization..  Organic letters,  5  ((20)):  (3595-3598).  [PMID:14507181]
3. Viktor Krchnák,Jaroslav Zajícek.  (2005-07-12)  Application of a dual linker with a reference cleavage site to discover a new reaction between amines and N-hydroxyphthalimide..  Journal of combinatorial chemistry,  7  ((4)):  (523-525).  [PMID:16004493]
4. Jian-fang Zou,Shao-qiu Sun,Yan-fei Li,Yu-jun Zhao,Yan-qing Pei,Guang-feng Liu.  (2006-11-14)  [Hydroxyphthalimide induced medicamentosa-like dermatitis in five patients]..  Zhonghua lao dong wei sheng zhi ye bing za zhi = Zhonghua laodong weisheng zhiyebing zazhi = Chinese journal of industrial hygiene and occupational diseases,  24  ((10)):  (625-625).  [PMID:17096955]
5. Enrico Baciocchi,Massimo Bietti,Massimo Di Fusco,Osvaldo Lanzalunga.  (2007-10-24)  A kinetic study of the electron-transfer reaction of the phthalimide-N-oxyl radical (PINO) with ferrocenes..  The Journal of organic chemistry,  72  ((23)):  (8748-8754).  [PMID:17949039]
6. V Krishnakumar,S Manohar,R Nagalakshmi.  (2008-01-26)  Crystal growth and characterization of N-hydroxyphthalimide (C8H5NO3) crystal..  Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy,  71  ((1)):  (110-115).  [PMID:18218335]
7. Juan Shen,Choon-Hong Tan.  (2008-10-31)  Anthrone-derived NHPI analogues as catalysts in reactions using oxygen as an oxidant..  Organic & biomolecular chemistry,  6  ((22)):  (4096-4098).  [PMID:18972037]
8. Sergiu Coseri,Gabriela Biliuta.  (2012-09-05)  Bromide-free oxidizing system for carboxylic moiety formation in cellulose chain..  Carbohydrate polymers,  90  ((4)):  (1415-1419).  [PMID:22944397]
9. Yuuki Amaoka,Shin Kamijo,Tamaki Hoshikawa,Masayuki Inoue.  (2012-11-02)  Radical amination of C(sp3)-H bonds using N-hydroxyphthalimide and dialkyl azodicarboxylate..  The Journal of organic chemistry,  77  ((22)):  (9959-9969).  [PMID:23113810]
10. Sergiu Coseri,Gabriela Biliuta,Bogdan C Simionescu,Karin Stana-Kleinschek,Volker Ribitsch,Valeria Harabagiu.  (2013-03-08)  Oxidized cellulose--survey of the most recent achievements..  Carbohydrate polymers,  93  ((1)):  (207-215).  [PMID:23465921]
11. M H Lang,O Hensel.  (1987-11-01)  [Contact allergy to dicyclohexylcarbodiimide and N-hydroxyphthalimide]..  Dermatosen in Beruf und Umwelt. Occupation and environment,  35  ((6)):  (212-213).  [PMID:2964358]
12. H M Petrassi,K B Sharpless,J W Kelly.  (2001-06-30)  The copper-mediated cross-coupling of phenylboronic acids and N-hydroxyphthalimide at room temperature: synthesis of aryloxyamines..  Organic letters,  3  ((1)):  (139-142).  [PMID:11429858]
13. Guanyu Yang,Yinfa Ma,Jie Xu.  (2004-08-26)  Biomimetic catalytic system driven by electron transfer for selective oxygenation of hydrocarbon..  Journal of the American Chemical Society,  126  ((34)):  (10542-10543).  [PMID:15327303]
14. S Coseri,G Nistor,L Fras,S Strnad,V Harabagiu,B C Simionescu.  (2009-09-03)  Mild and selective oxidation of cellulose fibers in the presence of N-hydroxyphthalimide..  Biomacromolecules,  10  ((8)):  (2294-2299).  [PMID:19722560]
15. Florence S Gaucher-Wieczorek,Ludovic T Maillard,Bernard Badet,Philippe Durand.  (2010-09-14)  Fluorous tagged N-hydroxy phthalimide for the parallel synthesis of O-aryloxyamines..  Journal of combinatorial chemistry,  12  ((5)):  (655-658).  [PMID:20831264]
16. Markus Tonigold,Ying Lu,Andreas Mavrandonakis,Angela Puls,Reiner Staudt,Jens M?llmer,Joachim Sauer,Dirk Volkmer.  (2011-06-21)  Pyrazolate-based cobalt(II)-containing metal-organic frameworks in heterogeneous catalytic oxidation reactions: elucidating the role of entatic states for biomimetic oxidation processes..  Chemistry (Weinheim an der Bergstrasse, Germany),  17  ((31)):  (8671-8695).  [PMID:21688331]
17. Riyuan Lin,Feng Chen,Ning Jiao.  (2012-08-03)  Metal-free, NHPI catalyzed oxidative cleavage of C-C double bond using molecular oxygen as oxidant..  Organic letters,  14  ((16)):  (4158-4161).  [PMID:22853190]
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