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[1,1'-双(二-苯基膦基)二茂铁]氯化钯(II),二氯甲烷复合物(1:1)

规格或纯度: 98%
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B119542-1g 1g 现货 Stock Image
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二茂铁 元素分类的化合物
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基本描述

规格或纯度 98%
英文名称 1,1'-Bis(diphenylphosphino)ferrocene-palladium dichloride dichloromethane adduct
别名 Umicore CX94;PdCl{2}(dppf)^.CH{2}Cl{2}
英文别名 Umicore CX94;[1,1'-Bis(diphenylphosphino)ferrocene]dichloropalladium Dichloromethane Adduct; Dichloro[1,1'-bis(diphenylphosphino)ferrocene]palladium Dichloromethane Adduct; [1,1'-Bis(diphenylphosphino)ferrocene]palladium chloride; PdCl{2}(dppf)^.CH{2}Cl{2
生化机理 Catalyst employed in the borylation of aryl halides with Bis(pinacolato)diboron as well as the coupling of the derived arylboronic esters with aryl halides leading to biaryls. Also used in the synthesis of lactams by CO insertion and medium-ring aryl ethers by intramolecular coupling of an aryl halide with an alcohol.
法律信息 Product of Umicore
储存温度 充氩
运输条件 常规运输
产品介绍

This product is useful for the borylation of triflate with pinacolborane.应用于钯催化交叉偶联反应

Application

This product is useful for the borylation of triflate with pinacolborane.
Application Guide for Palladium Catalyzed Cross-Coupling Reactions


Product class

M-P, Homogeneous Catalysts, Bidentate Ligands, Ferrocenyl Ligands - Achiral


Reaction type

Cross Coupling Reactions with Arenes, Carbonylation, Carboxylation, Alpha Arylation, Suzuki-Miyaura Coupling Reaction, Oxidation


Chemical properties

Chemical formula

C35H30Cl4FeP2Pd

Empirical formula

[Pd(dppf)Cl2]?x CH2Cl2

Molecular weight

816.65

Metal

Pd

Theoretical metal content

13

Physical state

crystalline

Color

red orange

名称和标识符

EC号 460-040-3
分子式

C34H28Cl2FeP2Pd.CH2Cl2
分子量 816.64

化学和物理性质

熔点 275-280°C

安全信息

象形图
ghs07

Harmful
危险声明 H315: Causes skin irritation
H319: Causes serious eye irritation
H335: May cause respiratory irritation
预防措施声明 P261,P305+P351+P338
WGK Germany 3

参考文献

1. Ján Cvengros,Jutta Schütte,Nils Schl?rer,J?rg Neud?rfl,Hans-Günther Schmalz.  (2009-07-11)  Electrophilic activation of benzaldehydes through ortho palladation: one-pot synthesis of 3-methylene-indan-1-ols through a domino allylstannylation/Heck reaction under neutral conditions..  Angewandte Chemie (International ed. in English),  48  ((33)):  (6148-6151).  [PMID:19591177]
2. Shunsuke Chiba,Yan-Jun Xu,Yi-Feng Wang.  (2009-08-25)  A Pd(II)-catalyzed ring-expansion reaction of cyclic 2-azidoalcohol derivatives: synthesis of azaheterocycles..  Journal of the American Chemical Society,  131  ((36)):  (12886-12887).  [PMID:19697931]
3. Oliver R Thiel,Michal M Achmatowicz,Andreas Reichelt,Robert D Larsen.  (2010-07-28)  Palladium-catalyzed coupling of aldehyde-derived hydrazones: practical synthesis of triazolopyridines and related heterocycles..  Angewandte Chemie (International ed. in English),  49  ((45)):  (8395-8398).  [PMID:20661974]
4. Leila Tabrizi, Hossein Chiniforoshan,.  (2017-10-07)  The cytotoxicity and mechanism of action of new multinuclear Scaffold Au.  Dalton transactions (Cambridge, England : 2003),  46  ((41)):  ( 14164-14173 ).  [PMID:28984321]
5. Sho Fujii,Ryo Ishimura,Atsushi Nakagawa,Noboru Kitamura.  (2017-10-24)  A novel multimode sensor showing cation-dependent fluorescence colour..  Physical chemistry chemical physics : PCCP,  19  ((42)):  (28943-28949).  [PMID:29058743]
6. Lixia Guo,Xiaoju Wang,Liheng Feng.  (2018-05-19)  Synthesis, photophysical and electrochemical properties of a blue emitter with binaphthalene and carbazole units..  Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy,  201  ():  (376-381).  [PMID:29775930]
7. Mikhail Feofanov,Arber Uka,Vladimir Akhmetov,Konstantin Amsharov.  (2020-04-29)  Photocyclization of diarylethylenes with a boronate moiety: a useful synthetic tool to soluble PAH building blocks..  Photochemical & photobiological sciences : Official journal of the European Photochemistry Association and the European Society for Photobiology,  19  ((5)):  (722-725).  [PMID:32342967]
8. Po-Hsuan Hsu,Sibidou Yougbaré,Jui-Chi Kuo,Dyah Ika Krisnawati,Achmad Jazidie,Mohammad Nuh,Po-Ting Chou,Yu-Cheng Hsiao,Tsung-Rong Kuo.  (2020-09-10)  One-Pot Synthesis of Thiol-Modified Liquid Crystals Conjugated Fluorescent Gold Nanoclusters..  Nanomaterials (Basel, Switzerland),  10  ((9)):  ().  [PMID:32899952]
9. Julien Monot,Malika Makhlouf Brahmi,Shau-Hua Ueng,Carine Robert,Marine Desage-El Murr,Dennis P Curran,Max Malacria,Louis Fensterbank,Emmanuel Lac?te.  (2009-10-06)  Suzuki-Miyaura coupling of NHC-boranes: a new addition to the C-C coupling toolbox..  Organic letters,  11  ((21)):  (4914-4917).  [PMID:19799407]
10. Wilfried Hess,Jonathan W Burton.  (2010-09-15)  Palladium-catalysed cyclisation of N-alkynyl aminomalonates..  Chemistry (Weinheim an der Bergstrasse, Germany),  16  ((41)):  (12303-12306).  [PMID:20839192]
11. Yameng Ren,Jiao Liu,Aibin Zheng,Xiandui Dong,Peng Wang.  (2017-09-22)  2.  Advanced science (Weinheim, Baden-Wurttemberg, Germany),  4  ((9)):  (1700099-1700099).  [PMID:28932672]
12. Zhaoyang Ding,Chunfei Wang,Shichao Wang,Li Wu,Xuanjun Zhang.  (2019-06-30)  Light-harvesting metal-organic framework nanoprobes for ratiometric fluorescence energy transfer-based determination of pH values and temperature..  Mikrochimica acta,  186  ((7)):  (476-476).  [PMID:31250248]
13. Zejun Li,Shumei Huang,Yong He,Qinya Duan,Guansheng Zheng,Yin Jiang,Lili Cai,Yongguang Jia,Huatang Zhang,Derek Ho.  (2020-01-25)  AND logic gate based fluorescence probe for simultaneous detection of peroxynitrite and hypochlorous acid..  Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy,  230  ():  (118073-118073).  [PMID:31978691]

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